
Answer: C. The reduction is \(\text{PbO} + \text{CO} \rightarrow \text{Pb} + \text{CO}_2\). Two requirements: identify the gaseous product, AND prevent excess CO escaping into the atmosphere.
Limewater identifies \(\text{CO}_2\) (turns milky → confirms reduction occurred). Collection of remaining gas over water in a downstream vessel traps any unreacted CO so it can't vent.
A uses concentrated sulfuric acid, which doesn't test for \(\text{CO}_2\). B has limewater but no second trap, so excess CO bubbles through and escapes. D applies limewater only at the final stage, after CO has already passed through earlier collection points.
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